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40 CFR § 133.104 - Sampling and test procedures.

---
identifier: "/us/cfr/t40/s133.104"
source: "ecfr"
legal_status: "authoritative_unofficial"
title: "40 CFR § 133.104 - Sampling and test procedures."
title_number: 40
title_name: "Protection of Environment"
section_number: "133.104"
section_name: "Sampling and test procedures."
chapter_name: "ENVIRONMENTAL PROTECTION AGENCY"
subchapter_number: "D"
subchapter_name: "WATER PROGRAMS"
part_number: "133"
part_name: "SECONDARY TREATMENT REGULATION"
positive_law: false
currency: "2026-04-05"
last_updated: "2026-04-05"
format_version: "1.1.0"
generator: "[email protected]"
authority: "Secs. 301(b)(1)(B), 304(d)(1), 304(d)(4), 308, and 501 of the Federal Water Pollution Control Act as amended by the Federal Water Pollution Control Act Amendments of 1972, the Clean Water Act of 1977, and the Municipal Wastewater Treatment Construction Grant Amendments of 1981; 33 U.S.C. 1311(b)(1)(B), 1314(d) (1) and (4), 1318, and 1361; 86 Stat. 816, Pub. L. 92-500; 91 Stat. 1567, Pub. L. 95-217; 95 Stat. 1623, Pub. L. 97-117."
regulatory_source: "49 FR 37006, Sept. 20, 1984, unless otherwise noted."
cfr_part: "133"
---

# 133.104 Sampling and test procedures.

(a) Sampling and test procedures for pollutants listed in this part shall be in accordance with guidelines promulgated by the Administrator in 40 CFR part 136.

(b) Chemical oxygen demand (COD) or total organic carbon (TOC) may be substituted for BOD<sub>5</sub> when a long-term BOD:COD or BOD:TOC correlation has been demonstrated.